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3-(Triethoxysilyl)propionitrile Sol-Gel Coating

Ying-Sing Li, Yun Xiao, Paul B Wright, Tuan Tran

Spectrochim Acta A Mol Biomol Spectrosc. 2005 May;61(7):1675-81.

PMID: 15820902

Abstract:

3-(Triethoxysilyl)propionitrile (TESPN) sol-gel has been prepared under different conditions. It was employed for coating the surfaces of quartz and aluminum. Infrared (IR) and Raman spectra of TESPN and TESPN sol-gels have been recorded in the study of the sol-gel process. Transmission and reflection absorption IR (RAIR) spectra of TESPN sol-gel coated quartz and aluminum have also been collected for better understanding the film formation on the substrate surfaces. Spectra collected at different temperatures indicated that the silane film on quartz decomposes at 700 degrees C. Results from thermal gravimetric analysis (TGA) supported this result. Based on the group frequencies and the spectral behavior in different states, some vibrational modes were assigned to the observed bands. The anticorrosion behavior of the sol-gel coated aluminum in comparison with the uncoated metal was evaluated by measuring the potentiodynamic polarization and electrochemical impedance spectra (EIS).

Chemicals Related in the Paper:

Catalog Number Product Name Structure CAS Number Price
AP919313 3-(Triethoxysilyl)propionitrile 3-(Triethoxysilyl)propionitrile 919-31-3 Price
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