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An unprecedented [{Fe 5 O 5(OH) 2(OAc) 2} 2{W 2 O 2(OH)}] cluster sandwiched in the tetravacant tungstophosphate

An unprecedented [{Fe 5 O 5(OH) 2(OAc) 2} 2{W 2 O 2(OH)}] cluster sandwiched in the tetravacant tungstophosphate

Zongfei Yang, Yaping Wang, Zhijie Liang, Jingkun Lu, Pengtao Ma, Jingyang Niu, Jingping Wang

Dalton Trans. 2019 Dec 7;48(45):16857-16860.

PMID: 31702746

Abstract:

A novel tungstophosphate H12Na4K3[{Fe5O5(OH)2(OAc)2}2{W2-O2(OH)}{P2W14O54}2]·36H2O (1) containing an unprecedented [{Fe5O5(OH)2(OAc)2}2{W2O2(OH)}] unit has been successfully obtained and characterized by IR, TGA, magnetic susceptibility measurements and single-crystal X-ray diffraction. It shows a decameric FeIII molecular assembly formed through two {Fe5O23} subunits bridged by a {W2O3} motif.

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