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[Determination of Cirsilineol in Herba Artemisiae Scopariae Collected in Autumn by HPLC]

[Determination of Cirsilineol in Herba Artemisiae Scopariae Collected in Autumn by HPLC]

Qi-wei Zhang, Yong-xin Zhang, Ying Zhang, Guo-gang Liang

Zhongguo Zhong Yao Za Zhi. 2002 Jan;27(1):23-5.

PMID: 12774348

Abstract:

Objective:
To establish a quantitative method for determination of cirsilineol in Herba Artemisiae Scopariae collected in Autumn.
Method:
Sample was extracted with methanol, and cleaned up with polyamide column. ODS column was used with methanol-acetonitrile-0.5% acetic acid solution (24:19:57) as mobile phase. Detection wavelength was 347 nm.
Result:
Cirsilineol in sample solution was well separated. Linearity of cirsilineol was good (r = 0.9998) in range of 0.1-0.8 microgram. The average recovery was 101.3%, RSD of repeatability was 3.04%.
Conclusion:
This method can be used for quality control of Herba Artemisiae Scopariae collected in autumn and its preparations.

Chemicals Related in the Paper:

Catalog Number	Product Name	Structure	CAS Number	Price
AP41365326	Cirsilineol		41365-32-6	Price

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