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Full Multinuclear Resonance Analysis of 4-amino-1,1,2,2,9,9,10,10-octafluoro[2.2]paracyclophane

Full Multinuclear Resonance Analysis of 4-amino-1,1,2,2,9,9,10,10-octafluoro[2.2]paracyclophane

Alex J Roche, Alexander A Marchione, Sheryl A Rabinowitz

Magn Reson Chem. 2005 Dec;43(12):1016-22.

PMID: 16142842

Abstract:

The complete assignment of 19F, 1H and 13C NMR spectra for a monosubstituted octafluoro[2.2]paracyclophane derivative is described for the first time. The unambiguous assignments were achieved through the combination of 19F--1H HOESY, 1H COSY and 19F COSY techniques and then further confirmed employing a complementary approach using a Karplus-dependent 3JCF interaction. Interesting aspects of the coupling patterns for various JHH, JHF, JCF and JFF interactions are also discussed.

Chemicals Related in the Paper:

Catalog Number	Product Name	Structure	CAS Number	Price
AP3345297	1,1,2,2,9,9,10,10-Octafluoro[2.2]paracyclophane		3345-29-7	Price

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