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GLC Determination of Alpha- And Beta-Tribenosides in Human Plasma

A Sioufi, F Pommier

J Pharm Sci. 1980 Feb;69(2):167-9.

PMID: 6892644

Abstract:

The determination of alpha-tribenoside at concentrations down to 10 ng/ml and beta-tribenoside at concentrations down to 5 ng/ml in human plasma is described. After addition of an internal standard, alpha- and beta-tribenosides are extracted at basic pH into benzene. Both compounds are derivatized with N-heptafluorobutyrylimidazole. The derivatives are determined by GLC using a 63Ni-electron-capture detector.

Chemicals Related in the Paper:

Catalog Number Product Name Structure CAS Number Price
AP32477353 N-Heptafluorobutyrylimidazole N-Heptafluorobutyrylimidazole 32477-35-3 Price
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