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Preparation of 6,6,1',1',6',6'-hexadeutero Sucrose

Preparation of 6,6,1',1',6',6'-hexadeutero Sucrose

Marie-Hélène Gouy, Mathieu Danel, Maud Gayral, Alain Bouchu, Yves Queneau

Carbohydr Res. 2007 Nov 5;342(15):2303-8.

PMID: 17640626

Abstract:

The preparation of 6,6,1',1',6',6'-hexadeutero sucrose is reported. The synthesis is based on a triple oxidation of a protected sucrose 6,1',6'-triol to the corresponding 6,1',6'-tricarboxylic acid or ester, followed by reduction with lithium aluminium deuteride. This triple oxidation could be achieved either using cat. TEMPO-NaOCl (to the acid) or PDC-Ac(2)O-t-BuOH (to the t-butyl carboxylic ester).

Chemicals Related in the Paper:

Catalog Number	Product Name	Structure	CAS Number	Price
AP13587161	Lithium deuteride		13587-16-1	Price

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