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Production of mono- to few-layer MoS 2 nanosheets in isopropanol by a salt-assisted direct liquid-phase exfoliation method

Production of mono- to few-layer MoS 2 nanosheets in isopropanol by a salt-assisted direct liquid-phase exfoliation method

Huaizhi Liu, Liao Xu, Weixu Liu, Bo Zhou, Yinyan Zhu, Lihua Zhu, Xiaoqing Jiang

J Colloid Interface Sci. 2018 Apr 1;515:27-31.

PMID: 29328941

Abstract:

Here, we report a facile salt-assisted direct liquid-phase exfoliation method for mass production of MoS2 nanosheets. We choose organic solvent isopropanol (IPA) as exfoliation media and potassium ferrocyanide, potassium sodium tartrate, or sodium tartrate as salt, the assistant. The selected salts show universal and efficient assistant effect for the exfoliation of MoS2 in IPA. Especially, potassium ferrocyanide (K4Fe(CN)6) can enhance the exfoliation efficiency up to 73 times and a dispersion of MoS2 nanosheets with concentration as high as 0.240 mg mL-1 can be easily obtained in IPA-K4Fe(CN)6 system. Transmission electron microscopy, atomic force microscopy (AFM), and Raman spectroscopy show that bulk MoS2 has been successfully exfoliated into mono- to few-layer MoS2 nanosheets. AFM analysis indicates that nearly 60% flakes are monolayer in MoS2 dispersion.

Chemicals Related in the Paper:

Catalog Number	Product Name	Structure	CAS Number	Price
AP6381595	Potassium sodium tartrate		6381-59-5	Price

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