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Synthesis and Characterization of Hybrid Materials Consisting of N-Octadecyltriethoxysilane by Using N-Hexadecylamine as Surfactant and Q(0) and T(0) Cross-Linkers

Synthesis and Characterization of Hybrid Materials Consisting of N-Octadecyltriethoxysilane by Using N-Hexadecylamine as Surfactant and Q(0) and T(0) Cross-Linkers

Ismail Warad, H Omar Abd-Elkader, Saud Al-Resayes, Ahmad Husein, Mohammed Al-Nuri, Ahmed Boshaala, Nabil Al-Zaqri, Taibi Ben Hadda

Int J Mol Sci. 2012;13(5):6279-91.

PMID: 22754364

Abstract:

Novel hybrid xerogel materials were synthesized by a sol-gel procedure. n-octadecyltriethoxysilane was co-condensed with and without different cross-linkers using Q(0) and T(0) mono-functionalized organosilanes in the presence of n-hexadecylamine with different hydroxyl silica functional groups at the surface. These polymer networks have shown new properties, for example, a high degree of cross-linking and hydrolysis. Two different synthesis steps were carried out: simple self-assembly followed by sol-gel transition and precipitation of homogenous sols. Due to the lack of solubility of these materials, the compositions of the new materials were determined by infrared spectroscopy, (13)C and (29)Si CP/MAS NMR spectroscopy and scanning electron microscopy.

Chemicals Related in the Paper:

Catalog Number	Product Name	Structure	CAS Number	Price
AP7399000	n-Octadecyltriethoxysilane		7399-00-0	Price

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