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Synthesis, Characterization and Application of N-Ti/13X/MCM-41 Mesoporous Molecular Sieves

Synthesis, Characterization and Application of N-Ti/13X/MCM-41 Mesoporous Molecular Sieves

Hong Tao, Nhat-Thien Nguyen, Xiao-Hui Hei, Cong Nguyen Nguyen, Hsiao-Hsin Tsai, I-Cheng Chang, Chang-Tang Chang

J Nanosci Nanotechnol. 2016 Jun;16(6):6567-74.

PMID: 27427754

Abstract:

Di-n-butyl phthalate (DBP) is a type of phthalate ester. In recent years, an increasing number of studies have examined the removal of DBP. In this study we use a composite material of N-Ti/13X/MCM-41, synthesized by nitrogen, molecular sieve 13X, tetrabutyl orthotitanate and tetraethyl orthosilicate as raw materials, CTAB as a structural template and tetrabutyl titanate and urea under hydrothermal conditions. The optimized experimental conditions, such as the amount of material, reaction time, pH value and initial concentration were tested. The surface areas of N-Ti/13X/MCM-41 were found to be 664 m2g(-1). TEM micrographs revealed N-Ti/13X/MCM-41 is consisting of aggregates of spherical particles, similar with standard synthesized MCM-41 (Mobil Composition of Matter No. 41). Through photocatalytic degradation experiments, the optimum degradation efficiency of DBP was more than 90% at a pH 6.0 with catalyst dosing of 0.15 g L(-1).

Chemicals Related in the Paper:

Catalog Number	Product Name	Structure	CAS Number	Price
AP4766578	Tetrabutyl orthosilicate		4766-57-8	Price

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