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Synthesis of a New Stable, Neutral organothulium(II) Complex by Reduction of a thulium(III) Precursor

Synthesis of a New Stable, Neutral organothulium(II) Complex by Reduction of a thulium(III) Precursor

Florian Jaroschik, François Nief, Louis Ricard

Chem Commun (Camb). 2006 Jan 28;(4):426-8.

PMID: 16493824

Abstract:

The new stable, neutral Tm(II) complex (Cp(ttt))2Tm [Cp(ttt) = 1,2,4-tris(tert-butyl)cyclopentadienyl] can be obtained either by direct reaction of NaCp(ttt) with TmI2 or by reduction of (Cp(ttt))2TmI in non-polar solvents; this latter route may prove itself useful for the isolation of other neutral non-classical low-valent organolanthanide species.

Chemicals Related in the Paper:

Catalog Number	Product Name	Structure	CAS Number	Price
AP1272260	Tris(cyclopentadienyl)thulium(III)		1272-26-0	Price

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