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The Facile and Efficient Synthesis of 8-chloroadenosine 3',5'-cyclic Monophosphate by Phosphorylative Cyclization of 8-chloroadenosine and Its Characterization by(1)H and (13)C NMR Spectroscopy

The Facile and Efficient Synthesis of 8-chloroadenosine 3',5'-cyclic Monophosphate by Phosphorylative Cyclization of 8-chloroadenosine and Its Characterization by(1)H and (13)C NMR Spectroscopy

N T Woo, S Y Jin, D J Cho, N S Kim, E H Bae, J H Jung, W H Ham, Y H Jung

Arch Pharm Res. 1997 Apr;20(2):176-9.

PMID: 18975197

Abstract:

Purine nucleosides were chlorinated by the reaction of acyl chloride in DMF with MCPBA under mild conditions with moderate yields. And, satisfactory method for the synthesis of ribonucleoside-3',5'-cyclic phosphates and its characterization by(1)H and(13)C nmr spectroscopy is described.

Chemicals Related in the Paper:

Catalog Number	Product Name	Structure	CAS Number	Price
AP41941564	8-Chloroadenosine 3′,5′-cyclic-monophosphate		41941-56-4	Price

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